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Table 1 Optimized heating program for GF AAS measurements

From: Aluminum concentrations in central and peripheral areas of malignant breast lesions do not differ from those in normal breast tissues

Step

Temperature

Ramp Time

Hold time

Flow rate

 

(°C)

(s)

(s)

(mL min − 1 )

Drying

110

1

30

250

Drying

130

15

30

250

Pyrolysis

1500

10

20

250

Atomization

2350

0

5

0

Cleaning

2450

1

3

250

Cooling

20

1

5

250

  1. Note: Correlation coefficients for Aluminum concentration and the water content of the samples were: 0.23 for normal tissues; 0.26 for peripheral tumor areas, and 0.16 for peripheral tumor areas, showing that samples with increased water content (and therefore lower fat content) had slightly higher concentrations of aluminum.